Metallacarboranes: Boron-Based Compounds Inhibit Key HIV Enzyme

 

Parimal M. Prajapati*, Yatri Shah, D.J. Sen and C.N. Patel

Department of Pharmaceutical and Medicinal Chemistry, Shri Sarvajanik Pharmacy College, Arvind Baug, Mehsana-384001, Gujarat, India. Phone:00-91-2762-247711, Fax:00-91-2762-247712

ABSTRACT:

Human immunodeficiency virus (HIV) is a lentivirus (a member of the retrovirus family) that causes acquired immunodeficiency syndrome (AIDS), a condition in humans in which the immune system begins to fail, leading to life-threatening opportunistic infections. Infection with HIV occurs by the transfer of blood, semen, vaginal fluid, pre-ejaculate, or breast milk. Within these bodily fluids, HIV is present as both free virus particles and virus within infected immune cells. The four major routes of transmission are unsafe sex, contaminated needles, breast milk, and transmission from an infected mother to her baby at birth. Metallacarboranes derived from the transition metals represent a large family of aromatic borane derivatives which, when equipped with a radiometal, are potentially useful in radioimaging and radiotherapy of tumors. The radiometallacarborane may be localized in tumor by a tumor cell-selective antibody molecule to which it is attached or by other means (biomolecule, liposome). A particular advantage of radiometallacarboranes in these applications is their extraordinarily great kinetic stability and invisibility to enzyme systems which normally degrade organic radiometal carriers (chelates) with release of the radiometal in an unwanted way.

 

INTRODUCTION

The genes of most living things, including humans, are made of DNA. The DNA exists as a sequence of a code that can be read like a book. In the cell the code is read to make RNA which is then used as the code for the construction of proteins. In other words, the flow of genetic information in the cell is usually from DNA to RNA to protein1.

 

FIGURE 1. HIV VIRUS

The HIV virus, on the other hand, has its genetic material made from RNA. It has to insert its genetic code into that of the host cell in order to replicate.


In order to achieve this it must first make a DNA copy so that it is compatible with the DNA of the host cell. DNA is then made using the code of the RNA. Since this is the opposite of the usual case the viruses that do this are called retroviruses2.

 

What does an HIV virus look like?

This is an artist's drawing of a single HIV virus. As you can see, the virus has several layers, including an outer layer, an inner layer and a core shell. The outer layer is interrupted by glycoproteins (gp) which play an important role in the lifecycle of the virus, and are targeted by a new type of drugs called "entry inhibitors". Within the core shell lies the genetic material of the virus (RNA), as well as some of the enzymes the virus needs to replicate. This includes Reverse Transcriptase, an enzyme that catalyzes the production of DNA based on the RNA genetic code. NRTI and NNRTI drugs inhibit the Reverse Transcriptase enzyme and thus prevent the virus from replicating3.

 

FIGURE.2  ANATOMY OF AIDS VIRUS

How does HIV live in humans?

HIV uses human cells, mainly white blood cells, as host cells to in which to replicate and thrive. The white blood cells that HIV uses as host cells are called CD4 T-lymphocytes, which are commonly called "CD4 cells" or "T-cells" for short. The numbers of these cells are what are referred to when someone discusses a "CD4 count," or a "T-cell count." CD4 cells are used to fight infection and are a key element of the immune system. In the process of replication, HIV kills CD4 cells. By replicating and killing CD4 cells, HIV degrades the immune system and renders the patient more4.

 

FIGURE 3: HIV USES HUMAN CELLS

What is AIDS?

HIV is present as both free virus particles and virus within infected immune cells. When CD4+ T cell numbers decline below a critical level of 200 cells per µL, cell-mediated immunity is lost, and infections with a variety of opportunistic microbes appear. The first symptoms often include moderate and unexplained weight loss, recurring respiratory tract infections (such as sinusitis, bronchitis, otitis media, pharyngitis),prostatitis, skin rashes, and oral ulcerations. Common opportunistic infections and tumors, most of which are normally controlled by robust CD4+ T cell-mediated immunity then start to affect the patient. Typically, resistance is lost early on to oral Candida species and to Mycobacterium tuberculosis, which leads to an increased susceptibility to oral candidiasis(thrush) and tuberculosis. Later, reactivation of latent herpes viruses may cause worsening recurrences of herpes simplex eruptions, shingles, Epstein-Barr virus-induced B-cell lymphomas, or Kaposi's sarcoma. Pneumonia caused by the fungus Pneumocystis jirovecii is common and often fatal. In the final stages of AIDS, infection with cytomegalovirus (another herpes virus) or Mycobacterium avium complex is more prominent. Not all patients with AIDS get all these infections or tumors, and there are other tumors and infections that are less prominent but still significant5.

 

Life Cycle of AIDS:

The HIV virus’s life cycle begins as it is born in a host cell. The virus exits the cell through its cell membrane, and searches for a new T-cell to infect. The virus can identify the cell it wishes to find, the CD4+ T-cell, because they have CD4 molecules on their surface. Once the virus reaches a victim, it attaches itself to the CD4 molecules that make up its surface, and the virus’s outer envelope merges with the cells and becomes one.

 

FIGURE. 4 LIFE CYCLE OF AIDS

After getting inside the cell, HIV uses a chemical called reverse transcriptase to convert RNA into DNA. This is the form of nucleic acid which can be used to produce copies of the virus.

When the DNA enters the cells nucleus, the next stage of the process is complete. This is done with the help of a chemical known as integrase. Next, the HIV DNA is turned into RNA that can use the cells machinery. After this is complete, this “messenger” RNA moves out of the nucleus and into the cytoplasm of the cell to take control of it. It creates proteins needed for more viruses using the host cells parts. The last stage occurs when these proteins join together and create young viruses. These are not yet ready to infect other cells. A chemical called protease cleans up the proteins and enzymes in these immature HIV strains, and then they gather up in the cells membrane and burst out. It is this eruption of new viruses that destroys the host cell 6-7

 

What is the treatment for HIV or AIDS?

Every person is different and your doctor will design a specific medical plan for you. It is essential that you follow this plan exactly, taking your medications exactly as prescribed. Some of the medications you will receive are intended to fight opportunistic infections. Other medications target the HIV virus in order to block replication and protect the body's immune system. These drugs are called "antiretroviral drugs." Often several antiretroviral drugs are prescribed for maximum effect. This is sometimes called "cocktail" therapy or highly active antiretroviral therapy (HAART). HIV protease (PR) represents a prime target for rational drug design, and protease inhibitors (PI) are powerful antiviral drugs. Most of the current PIs are pseudopeptide compounds with limited bioavailability and stability, and their use is compromised by high costs, side effects, and development of resistant strains. In our search for novel PI structures, we have identified a group of inorganic compounds, icosahedral metallacarboranes, as candidates for a novel class of nonpeptidic PIs. Here, we report the potent, specific, and selective competitive inhibition of HIV PR by substituted metallacarboranes. The most active compound, sodium hydrogen butylimino bis-8,8-[5-(3-oxa-pentoxy)-3-cobalt bis(1,2-dicarbollide)]di-ate, exhibited a K i value of 2.2 nM and a submicromolar EC50 in antiviral tests, showed no toxicity in tissue culture, weakly inhibited human cathepsin D and pepsin, and was inactive against trypsin, papain, and amylase. The structure of the parent cobalt bis(1,2-dicarbollide) in complex with HIV PR was determined at 2.15 Ĺ resolution by protein crystallography and represents the first carborane-protein complex structure determined. It shows the following mode of PR inhibition: two molecules of the parent compound bind to the hydrophobic pockets in the flap-proximal region of the S3 and S3′ subsites of PR. We suggest, therefore, that these compounds block flap closure in addition to filling the corresponding binding pockets as conventional PIs. This type of binding and inhibition, chemical and biological stability, low toxicity, and the possibility to introduce various modifications make boron clusters attractive pharmacophores for potent and specific enzyme inhibition 8-9.

 

FIGURE.5 A metallacarborane-based molecular motor devised lab rotates by charge transfer and is stabilized by a hydrogen bond.


Metallacarboranes and Related Species as Radionuclide Carriers for Antibody-Mediated  Diagnosis and Therapy

Metallacarboranes derived from the transition metals represent a large family of aromatic borane derivatives which, when equipped with a radiometal, are potentially useful in radioimaging and radiotherapy of tumors. The radiometallacarborane may be localized in tumor by a tumor cell-selective antibody molecule to which it is attached or by other means (biomolecule, liposome). A particular advantage of radiometallacarboranes in these applications is their extraordinarily great kinetic stability and invisibility to enzyme systems which normally degrade organic radiometal carriers (chelates) with release of the radiometal in an unwanted way. The space-filling model shown below is a representation of a radiometallacarborane utilizing a generalized Co3+ nucleus and the Venus Flytrap ligand system which is, in turn, connected to a tumor-selective antibody. Use of 55Co, a positron emitter, is under investigation for application as a positron emission tomography (PET) agent. PET is extraordinarily useful in diagnosis. Other radioimaging systems based upon the invincibility of aromatic boranes to enzyme attack involve simple radioiodination of the ubiquitous nido-7,8-C2B9H12- ion and its derivatives. This is a facile process and the iodine remains fixed to the boron atom to which it is bound. These and other useful systems are described in M. Frederick Hawthorne and Andreas Maderna, "Applications of Radiolabeled Boron Clusters to the Diagnosis and Boron Neutron Capture Therapy of Cancer," Chem. Rev., 99, 3421 (1999). The use of radionuclides which emit alpha or beta particles would be useful as therapeutic agents against cancer and work of this type is also underway. Enzymes are protein molecules which catalyze important chemical reactions in our body. To perform their action, enzymes bind to other molecules called ligands or substrates. Sometimes, enzymes must be blocked to prevent them to cause diseases, like in the case of HIV-1 protease which is involved in AIDS. A small ligand (drug) is therefore designed which binds to the enzyme blocking it.10-12.

 

Preparation of Metallacarboranes

1) Compounds of the type shown in FIG. 1 were prepared by the reaction of the tetrathallium salt of “Z compound” shown in FIG. 8C with two equivalents of (Ph 3 P) 2 HCl 2 (where M=Pt, Pd, Co, Ni) in dry THF at room temperature under dry nitrogen conditions for 1 hour (reaction appeared to be complete after about 10 minutes). The TlCl precipitated, leaving the desired product in solution. This air-stable product was filtered and pumped to dryness in vacuo giving yields of 40-75%. Compounds were characterised by IR, NMR, elemental analysis, mass spectrometry and magnetic measurements. By way of example, Tl 4 [1,4-(1-C 6 H 5 —C 2 B 9 H 9 ) 2 C 6 H 4 ] (328 mg, 0.25 mmol) was suspended in stirred thf (40 ml) under ambient conditions, and brown (PPh 3 ) 2 Col 2 (420 mg, 0.50 mmol) was added. This immediately caused the formation of an off-white precipitate (Thallium (I) iodide), which turned grey on standing in air. After 30 minutes stirring, the bright green solution was isolated by filtration and the thf removed in vacuo, yielding Bis-Co (PPh 3 ) 2 -1,4-(1-C 5 H 5 —C 2 B 9 H 9 ) 2 C 6 . Appearance: Bright green powder Yield: 311 mg, 75% boron-containing compound can inhibit HIV protease, a key enzyme involved in replicating the virus that causes Aids. The finding is potentially signficant because the compounds - metallacarboranes - attack the enzyme in a different way to most existing drugs and could help overcome problems of resistance. Carboranes are polyhedral cages composed of carbon and boron atoms. The cages can be paired through a metal ion - in this case cobalt - to form metallacarboranes. linked two of these pairs together using a short chain with a quaternary amine in the centre. A range of these compounds with different substituents attached to the quaternary amine, and tested their effect on HIV protease in the test tube 13-15.

The team found that significant inhibition of the enzyme could be achieved - with varying degrees of potency depending on the nature of the substituent groups on the amine. Importantly the compounds also inhibited variants of the enzyme that had developed resistance to existing treatments16.

 

FIGURE.6 TWO METABLLOBORANES ARE JOINED BY A LINKER CHAIN WITH A CENTRAL QUATERNARY AMINE

 

X-ray structure of how the compounds bind to HIV protease

 

X-ray crystallography of the inhibitor binding to the enzyme showed that the while the molecules were occupying the enzyme's active site, the same as existing drugs and the natural peptide, the metallacarborane cages additionally interfered with other key parts of the enzyme's structure. Based on these findings that metallacarboranes are worth pursuing as HIV protease inhibitors. 'Their chemical and biological stability, low toxicity, and the possibility to introduce heteroatoms into the cage or polar group modifications to the side chains make boron clusters very attractive pharmacophores for development of potent HIV protease inhibitors 17-19.

 

FIGURE.7 X-RAY STRACTURE ANALYSIS OF THE BINDING OF COMPOUND TO HIV-PR.

 

 (A) Overall structure of the HIV PR-compound complex. The PR dimer is in ribbon representation with the two catalytic aspartates shown in sticks. Two compound molecules are represented by their van der Waals surfaces and gray stick model, with cobalt ions shown as magenta spheres. Autoproteolytic peptide product is represented as stick model. (B)  Superposition of PR-compound complex with PR-lopinavir complex and with the free PR structure. Protease complex with lopinavir  is represented in yellow ribbons, lopinavir is shown as a stick model, free PR structure (PDB ID code 1HHP) is shown in green  ribbons, and color coding for PR-compound  complex is the same     in  A 20-21 .

 

CONCLUSION:

Metallacarboranes are worth pursuing as HIV protease inhibitors. 'Their chemical and biological stability, low toxicity, and the possibility to introduce heteroatoms into the cage or polar group modifications to the side chains make boron clusters very attractive pharmacophores for development of potent HIV protease inhibitors. A particular advantage of radiometallacarboranes in these applications is their extraordinarily great kinetic stability and invisibility to enzyme systems which normally degrade organic radiometal carriers (chelates) with release of the radiometal in an unwanted way.

 

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Received on 27.01.2010

Accepted on 20.03.2010     

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Research J. Pharmacology and Pharmacodynamics. 2(3): May-June 2010, 205-210